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Peptide purity testing: HPLC & mass spectrometry

How HPLC and mass spectrometry characterize the purity and identity of research peptides.

By TagPep Editorial Team · Published June 6, 2026 · Updated June 9, 2026

How research peptides are characterized

Two analytical methods are commonly used to characterize research peptides: high-performance liquid chromatography (HPLC) and mass spectrometry (MS).

HPLC — purity

HPLC separates the components of a sample as they pass through a column, producing a chromatogram. The relative size of the main peak versus other peaks is used to estimate purity — how much of the sample is the target compound versus impurities.

Mass spectrometry — identity

Mass spectrometry measures the mass-to-charge ratio of ionized molecules, helping confirm a compound molecular weight and identity. It answers "is this the right molecule?" where HPLC answers "how pure is it?"

Reading the results

  • A higher main-peak percentage on HPLC indicates higher purity.
  • An MS result matching the expected mass supports correct identity.
  • Methods and acceptance criteria vary by compound.

Frequently asked

What purity is typical?

It varies by compound and supplier. Review the reported value on the batch-specific COA.

Does testing make a product safe to use?

No. Testing characterizes the material for research reference only. Products are not for human or veterinary use.

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Educational content for research reference only — not medical, veterinary, or personal-use advice. Products referenced are research compounds supplied for laboratory research use only and are not intended for human or veterinary use.